SOP Repository

SOPCategoryAuthorDate SubmittedKeywords
RecrystallizationReaction SetupMiller Group (UNC)2016-04-27Crystals, solvent mixtures
Aqua RegiaCleaningMiller Group (UNC)2016-07-14aqua regia, cleaning, glassware
Base BathCleaningMiller Group (UNC)2016-07-14base, cleaning, glassware
Carbon MonoxideReaction SetupMiller Group (UNC)2016-07-14CO, carbon monoxide, gases
WasteCleaningMiller Group (UNC)2016-07-24waste
Vacuum TransferReaction SetupMiller Group (UNC)2016-07-24vacuum, air-free manipulations
Solvent Purification: Solvent SystemInstrumentMiller Group (UNC)2016-07-24solvent purification
RotovapInstrumentMiller Group (UNC)2016-07-24vacuum, evaporation
Pyrophoric ChemicalsReaction SetupMiller Group (UNC)2016-07-24pyrophorics, flammable, air-free manipulations
Pressure Reactor: Parr Multi-reactorInstrumentMiller Group (UNC)2016-07-24pressure, reactor
Liquid OxygenReaction SetupMiller Group (UNC)2016-07-24oxygen, LO2, safety, air-free manipulatoins
Lecture BottlesReaction SetupMiller Group (UNC)2016-07-24pressure, gases
Laboratory NotebookReaction SetupMiller Group (UNC)2016-07-24notebook
Solvent Purification: Ketyl Radical TestReaction SetupMiller Group (UNC)2016-07-24water content, dry solvents
IR SpectroscopyInstrumentMiller Group (UNC)2016-07-24infrared, IR, spectroscopy
Inorganic Reaction WorkupReaction SetupMiller Group (UNC)2016-07-24workup, purification
Glovebox: RegenerationInstrumentMiller Group (UNC)2016-07-24glovebox, air-free manipulations
Glovebox: Antechamber UsageInstrumentMiller Group (UNC)2016-07-24glovebox, air-free manipulations
Gas Cylinder UsageReaction SetupMiller Group (UNC)2016-07-24pressure, gases
Electrochemistry: Electrode PolishingInstrumentMiller Group (UNC)2016-07-24electrochemistry
Electrochemistry: TroubleshootingInstrumentMiller Group (UNC)2016-07-24electrochemistry
Solvent Purification: DegassingReaction SetupMiller Group (UNC)2020-02-06Degassing
Cleaning GlasswareCleaningMiller Group (UNC)2024-07-05cleaning, glassware
Vacuum Pumps: Changing OilInstrumentMiller Group (UNC)2016-07-24vacuum, oil
Chemical Waste ManifestationCleaningTonks Group (UMN)2017-07-09Waste
Vendors and Technical Support</a.InstrumentTonks Group (UMN)2017-07-09Technical, Vendors
Solvent PotsReaction SetupTonks Group (UMN)2017-07-09Solvent, Distillation
Safe Operating Cards (SOCs)Reaction SetupTonks Group (UMN)2017-07-09Safety, Communication
High Pressure Reactors: Parr VesselReaction SetupTonks Group (UMN)2017-07-09Pressure, reactor
Lab Safety OverviewGeneralTonks Group (UMN)2017-07-09Safety
Laboratory NotebookReaction SetupTonks Group (UMN)2017-07-09Notebook
Group MeetingsGeneralTonks Group (UMN)2017-07-09Meetings
Group CleanupCleaningTonks Group (UMN)2017-07-09Safety, Cleanup
Freeze-Pump-Thaw DegassingReaction SetupTonks Group (UMN)2017-07-09Degassing
High Pressure Reactors: Fisher-Porter BottlesReaction SetupTonks Group (UMN)2017-07-09Pressure, reactor
Laboratory ExpectationsGeneralTonks Group (UMN)2017-07-09Safety, Communication
Cleaning GlasswareCleaningTonks Group (UMN)2017-07-09Glassware, cleaning
Chemical StorageGeneralTonks Group (UMN)2017-07-09Storage, Compatibility
Laboratory CheckoutGeneralTonks Group (UMN)2017-07-09Checkout, exit
Characterizing CompoundsReaction SetupTonks Group (UMN)2017-07-09Spectroscopy, characterization
Vacuum TrapsInstrumentMiller Group (UNC)2017-09-25Vacuum, air-free
Elemental Analysis and Sealing AmpulesGeneralMiller Group (UNC)2018-05-28Analysis, sealing, ampoules, ampules
OceanOptics Filewriter for KineticsInstrumentMiller Group (UNC)2018-06-30Spectroscopy, kinetics, reaction monitoring
Workup for Ni reactions under COReaction SetupMiller Group (UNC)2018-06-30Pressure, reactor, carbon monoxide
NMR: Non-Uniform SamplingInstrumentMiller Group (UNC)2018-09-02NMR Spectroscopy
NMR: Absolute Heteronuclei ReferencingInstrumentMiller Group (UNC)2018-09-02NMR Spectroscopy
Liquid DispensingReaction SetupMiller Group (UNC)2018-09-04Pipet, Syringe, Cannula, Addition funnel, Volumetric
SDS GuideGeneralMiller Group (UNC)2019-02-14SDS, hazard assessment
ShippingGeneralMiller Group (UNC)2020-02-06Shipping, mail
Electrochemistry: Aqueous Silver Reference ElectrodesElectrochemistryMiller Group (UNC)2021-10-08Electrochemistry
Electrochemistry: Electrode PolishingElectrochemistryMiller Group (UNC)2021-11-19Electrochemistry, Electrodes
Electrochemistry: Cyclic VoltammetryElectrochemistryMiller Group (UNC)2021-11-19Electrochemistry, CV
Electrochemistry: Controlled Potential ElectrolysisElectrochemistryYang Group (UCI) and Miller Group (UNC)2022-01-12Electrochemistry
Stoichiometric Gas AdditionsReaction SetupSaouma Group (Utah)2022-07-10gases, Schlenk technique
Glovebox Group ManualReaction SetupMiller Group (UNC)2023-04-18Glovebox, inert atmosphere, instrumentation
BalancesReaction SetupMiller Group (UNC)2024-07-05Weighing materials
Acid BathCleaningMiller Group (UNC)2024-07-05Cleanup, glassware
Drying Alumina, Sieves, CeliteGeneralMiller Group (UNC)2024-07-05Drying
HEL Multi-ReactorReaction Setup Miller Group (UNC)2024-07-05High pressure reactions, reactor
Synthesis of NaBArF4Reaction SetupMiller Group (UNC)2024-07-05Synthetic procedure
DFT Workflow & TroubleshootingComputation / DFTMiller Group (UNC)2024-08-22Computational methods
DFT Intrinsic Bonding Orbital AnalysisComputation / DFTMiller Group (UNC)2024-08-22Computational methods
Fume Hood Sensor CalibrationInstrumentMiller Group (UNC)2024-08-23Fume hoods, ventilation, sensors