Recrystallization | Reaction Setup | Miller Group (UNC) | 2016-04-27 | Crystals, solvent mixtures |
Aqua Regia | Cleaning | Miller Group (UNC) | 2016-07-14 | aqua regia, cleaning, glassware |
Base Bath | Cleaning | Miller Group (UNC) | 2016-07-14 | base, cleaning, glassware |
Carbon Monoxide | Reaction Setup | Miller Group (UNC) | 2016-07-14 | CO, carbon monoxide, gases |
Waste | Cleaning | Miller Group (UNC) | 2016-07-24 | waste |
Vacuum Transfer | Reaction Setup | Miller Group (UNC) | 2016-07-24 | vacuum, air-free manipulations |
Solvent Purification: Solvent System | Instrument | Miller Group (UNC) | 2016-07-24 | solvent purification |
Rotovap | Instrument | Miller Group (UNC) | 2016-07-24 | vacuum, evaporation |
Pyrophoric Chemicals | Reaction Setup | Miller Group (UNC) | 2016-07-24 | pyrophorics, flammable, air-free manipulations |
Pressure Reactor: Parr Multi-reactor | Instrument | Miller Group (UNC) | 2016-07-24 | pressure, reactor |
Liquid Oxygen | Reaction Setup | Miller Group (UNC) | 2016-07-24 | oxygen, LO2, safety, air-free manipulatoins |
Lecture Bottles | Reaction Setup | Miller Group (UNC) | 2016-07-24 | pressure, gases |
Laboratory Notebook | Reaction Setup | Miller Group (UNC) | 2016-07-24 | notebook |
Solvent Purification: Ketyl Radical Test | Reaction Setup | Miller Group (UNC) | 2016-07-24 | water content, dry solvents |
IR Spectroscopy | Instrument | Miller Group (UNC) | 2016-07-24 | infrared, IR, spectroscopy |
Inorganic Reaction Workup | Reaction Setup | Miller Group (UNC) | 2016-07-24 | workup, purification |
Glovebox: Regeneration | Instrument | Miller Group (UNC) | 2016-07-24 | glovebox, air-free manipulations |
Glovebox: Antechamber Usage | Instrument | Miller Group (UNC) | 2016-07-24 | glovebox, air-free manipulations |
Gas Cylinder Usage | Reaction Setup | Miller Group (UNC) | 2016-07-24 | pressure, gases |
Electrochemistry: Electrode Polishing | Instrument | Miller Group (UNC) | 2016-07-24 | electrochemistry |
Electrochemistry: Troubleshooting | Instrument | Miller Group (UNC) | 2016-07-24 | electrochemistry |
Solvent Purification: Degassing | Reaction Setup | Miller Group (UNC) | 2020-02-06 | Degassing |
Cleaning Glassware | Cleaning | Miller Group (UNC) | 2024-07-05 | cleaning, glassware |
Vacuum Pumps: Changing Oil | Instrument | Miller Group (UNC) | 2016-07-24 | vacuum, oil |
Chemical Waste Manifestation | Cleaning | Tonks Group (UMN) | 2017-07-09 | Waste |
Vendors and Technical Support</a. | Instrument | Tonks Group (UMN) | 2017-07-09 | Technical, Vendors |
Solvent Pots | Reaction Setup | Tonks Group (UMN) | 2017-07-09 | Solvent, Distillation |
Safe Operating Cards (SOCs) | Reaction Setup | Tonks Group (UMN) | 2017-07-09 | Safety, Communication |
High Pressure Reactors: Parr Vessel | Reaction Setup | Tonks Group (UMN) | 2017-07-09 | Pressure, reactor |
Lab Safety Overview | General | Tonks Group (UMN) | 2017-07-09 | Safety |
Laboratory Notebook | Reaction Setup | Tonks Group (UMN) | 2017-07-09 | Notebook |
Group Meetings | General | Tonks Group (UMN) | 2017-07-09 | Meetings |
Group Cleanup | Cleaning | Tonks Group (UMN) | 2017-07-09 | Safety, Cleanup |
Freeze-Pump-Thaw Degassing | Reaction Setup | Tonks Group (UMN) | 2017-07-09 | Degassing |
High Pressure Reactors: Fisher-Porter Bottles | Reaction Setup | Tonks Group (UMN) | 2017-07-09 | Pressure, reactor |
Laboratory Expectations | General | Tonks Group (UMN) | 2017-07-09 | Safety, Communication |
Cleaning Glassware | Cleaning | Tonks Group (UMN) | 2017-07-09 | Glassware, cleaning |
Chemical Storage | General | Tonks Group (UMN) | 2017-07-09 | Storage, Compatibility |
Laboratory Checkout | General | Tonks Group (UMN) | 2017-07-09 | Checkout, exit |
Characterizing Compounds | Reaction Setup | Tonks Group (UMN) | 2017-07-09 | Spectroscopy, characterization |
Vacuum Traps | Instrument | Miller Group (UNC) | 2017-09-25 | Vacuum, air-free |
Elemental Analysis and Sealing Ampules | General | Miller Group (UNC) | 2018-05-28 | Analysis, sealing, ampoules, ampules |
OceanOptics Filewriter for Kinetics | Instrument | Miller Group (UNC) | 2018-06-30 | Spectroscopy, kinetics, reaction monitoring |
Workup for Ni reactions under CO | Reaction Setup | Miller Group (UNC) | 2018-06-30 | Pressure, reactor, carbon monoxide |
NMR: Non-Uniform Sampling | Instrument | Miller Group (UNC) | 2018-09-02 | NMR Spectroscopy |
NMR: Absolute Heteronuclei Referencing | Instrument | Miller Group (UNC) | 2018-09-02 | NMR Spectroscopy |
Liquid Dispensing | Reaction Setup | Miller Group (UNC) | 2018-09-04 | Pipet, Syringe, Cannula, Addition funnel, Volumetric |
SDS Guide | General | Miller Group (UNC) | 2019-02-14 | SDS, hazard assessment |
Shipping | General | Miller Group (UNC) | 2020-02-06 | Shipping, mail |
Electrochemistry: Aqueous Silver Reference Electrodes | Electrochemistry | Miller Group (UNC) | 2021-10-08 | Electrochemistry |
Electrochemistry: Electrode Polishing | Electrochemistry | Miller Group (UNC) | 2021-11-19 | Electrochemistry, Electrodes |
Electrochemistry: Cyclic Voltammetry | Electrochemistry | Miller Group (UNC) | 2021-11-19 | Electrochemistry, CV |
Electrochemistry: Controlled Potential Electrolysis | Electrochemistry | Yang Group (UCI) and Miller Group (UNC) | 2022-01-12 | Electrochemistry |
Stoichiometric Gas Additions | Reaction Setup | Saouma Group (Utah) | 2022-07-10 | gases, Schlenk technique |
Glovebox Group Manual | Reaction Setup | Miller Group (UNC) | 2023-04-18 | Glovebox, inert atmosphere, instrumentation |
Balances | Reaction Setup | Miller Group (UNC) | 2024-07-05 | Weighing materials |
Acid Bath | Cleaning | Miller Group (UNC) | 2024-07-05 | Cleanup, glassware |
Drying Alumina, Sieves, Celite | General | Miller Group (UNC) | 2024-07-05 | Drying |
HEL Multi-Reactor | Reaction Setup | Miller Group (UNC) | 2024-07-05 | High pressure reactions, reactor |
Synthesis of NaBArF4 | Reaction Setup | Miller Group (UNC) | 2024-07-05 | Synthetic procedure |
DFT Workflow & Troubleshooting | Computation / DFT | Miller Group (UNC) | 2024-08-22 | Computational methods |
DFT Intrinsic Bonding Orbital Analysis | Computation / DFT | Miller Group (UNC) | 2024-08-22 | Computational methods |
Fume Hood Sensor Calibration | Instrument | Miller Group (UNC) | 2024-08-23 | Fume hoods, ventilation, sensors |